Nmr Imaging of Materials

by
Edition: Reprint
Format: Paperback
Pub. Date: 2003-03-27
Publisher(s): Clarendon Press
List Price: $128.00

Buy New

Usually Ships in 5-7 Business Days
$127.36

Rent Textbook

Select for Price
There was a problem. Please try again later.

Rent Digital

Online: 180 Days access
Downloadable: 180 Days
$87.75
Online: 365 Days access
Downloadable: 365 Days
$101.25
Online: 1460 Days access
Downloadable: Lifetime Access
$134.99
$87.75

Used Textbook

We're Sorry
Sold Out

Summary

NMR imaging of materials is a field of increasing importance. Applications expand from fundamental science like the characterization of fluid transport in porous rock, catalyst pellets and hemodialyzers into various fields of engineering for process optimization and product and quality control, for example, of polymer materials, biomaterials, elastomers, and ceramics. While the results of NMR imaging are being appreciated in a growing community, the methods of imaging are far more diverse for materials applications that for medical imaging of humans. This book provides an introduction to NMR imaging of materials covering solid-state NMR spectroscopy, imaging methods for liquid and solid samples and unusual NMR in terms of special approaches to spatial resolution like an NMR surface scanner. SPecial attention is paid to the large variety of ways to generate image contrast-the most prominent feature of NMR. The text is strong on methodology, and includes today's important application areas.

Table of Contents

List of symbols and abbreviations
xv
Introduction
1(16)
Nuclear magnetic resonance
1(11)
NMR and the spinning top
2(1)
NMR spectroscopy
3(2)
NMR imaging
5(3)
NMR imaging in biomedicine
8(1)
Contrast in NMR imaging
8(1)
NMR imaging in materials science
9(2)
Equipment
11(1)
About this book
12(5)
The NMR signal in the presence of slow molecular motion
12(3)
Literature
15(1)
The contents of this book
15(2)
Fundamentals
17(50)
Magnetic fields
17(5)
Homogeneous magnetic fields
18(1)
Magnetic-field gradients
19(3)
Principles of NMR
22(29)
An NMR primer
23(21)
Spin-system response from quantum mechanics
44(7)
Hardware
51(16)
Overview of basic components
51(1)
The magnet
52(4)
The transmitter side
56(5)
The receiver side
61(6)
NMR spectroscopy
67(58)
Anisotropic nuclear spin interactions
69(10)
Interaction Hamiltonians
69(5)
General formalism
74(1)
Strong magnetic fields
75(3)
Orientation dependence of the resonance frequency
78(1)
Wideline NMR
79(12)
Molecular order
80(5)
Molecular reorientation
85(6)
High-resolution solid-state NMR
91(21)
Cross-polarization
92(4)
High-power decoupling
96(1)
Sample spinning
96(11)
Multi-pulse methods
107(5)
Echoes
112(6)
Relaxation
118(7)
Liquids
118(3)
Solids and slow motion
121(2)
Spin diffusion
123(2)
Transformation, convolution, and correlation
125(19)
Fourier transformation
126(3)
Convolution
129(4)
Linear systems
129(1)
Nonlinear systems
130(2)
The convolution theorem
132(1)
Correlation
133(2)
Linear system analysis
133(1)
Nonlinear cross-correlation
134(1)
The correlation theorem
135(1)
Further transformations
135(9)
Laplace transformation
136(1)
Hankel transformation
136(1)
Abel transformation
137(2)
z transformation
139(1)
Hadamard transformation
139(2)
Wavelet transformation
141(3)
Concepts of spatial resolution
144(55)
Point methods
145(3)
FONAR
145(2)
The sensitive-point method
147(1)
Line methods
148(1)
The multiple sensitive-point method
148(1)
Line-scan methods using selective excitation
148(1)
Selective excitation
148(21)
Excitation and response
151(3)
Shaped pulses
154(6)
Composite pulses
160(3)
Pulse sequences
163(3)
Solid-state techniques
166(3)
Magnetization in field gradients
169(30)
Linear and nonlinear responses
170(3)
Position: k space
173(5)
Velocity: q space
178(17)
Acceleration: ε space
195(4)
Basic imaging methods
199(45)
Reconstruction from projections
200(8)
Fourier imaging
208(23)
The spin-warp technique
208(5)
Multi-slice imaging
213(1)
3D imaging
214(1)
Spectroscopic imaging
215(3)
Stimulated-echo imaging
218(3)
Imaging with CPMG echoes
221(2)
Gradient-echo imaging
223(1)
Ultra-fast imaging
224(7)
Imaging in the rotating frame
231(4)
Imaging with noise excitation
235(9)
Contrast
244(85)
Image contrast
245(17)
Optimization of contrast
245(1)
Magnetization filters: parameter weights
246(1)
Transfer functions and mobility filters
246(2)
Parameter contrast
248(4)
Contrast parameters
252(1)
NMR parameters and material properties
253(9)
Filters
262(53)
T1 filters
263(3)
T2 filters
266(2)
T1p filters
268(2)
Chemical-shift filters
270(3)
Susceptibility contrast
273(3)
Translational diffusion and transport filters
276(12)
Local-field filters
288(6)
Combination filters
294(3)
Morphology filters
297(3)
Multi-quantum filters
300(7)
Homonuclear magnetization-transfer filters
307(3)
Heteronuclear magnetization-transfer filters
310(5)
Spectroscopic parameters
315(8)
1D spectroscopy
316(4)
Multi-dimensional spectroscopy
320(3)
Sample manipulation
323(6)
Temperature variation
324(1)
Magnetic field distortions
324(2)
Contrast agents
326(1)
Noble gases
327(2)
Solid-state NMR imaging
329(49)
Stray-field imaging
330(5)
Imaging with oscillating gradients
335(4)
Imaging with pure phase encoding
339(6)
Multi-quantum imaging
345(7)
MAS imaging
352(8)
Magic-angle rotating-frame imaging
360(3)
Imaging with multi-pulse line narrowing
363(7)
Principle
364(2)
Methods
366(4)
Imaging with magic echoes
370(8)
Multi-pulse sequences from magic echoes
371(4)
Magic-echo phase encoding
375(3)
Spatially resolved NMR
378(46)
Gradient methods
379(10)
Single-shot techniques
380(7)
Multi-shot techniques
387(2)
Surface-coil methods
389(12)
Theory of surface coils
390(6)
Working with inhomogeneous B1 fields
396(5)
Dedicated NMR
401(23)
Experimental aspects
402(6)
On-line coupling of high-resolution NMR
408(2)
Geophysical exploration
410(5)
Single-sided NMR
415(9)
Applications
424(45)
Fluid matter
425(14)
Oscillating reactions
425(2)
Flow and diffusion: rock cores, chromatography columns, and complex fluids
427(8)
Fluid ingress into polymers
435(3)
Current-density imaging
438(1)
Soft matter
439(16)
Defects in technical elastomers
440(4)
Stress and strain in elastomer materials
444(5)
Green-state ceramics
449(3)
Chemical-shift imaging of plants
452(3)
Hard matter: Polymers
455(14)
Spectroscopic and chemical-shift selective imaging
456(4)
Relaxation and spin-diffusion parameter imaging
460(9)
References
469(57)
Chapter 1
469(2)
Chapter 2
471(3)
Chapter 3
474(4)
Chapter 4
478(2)
Chapter 5
480(5)
Chapter 6
485(5)
Chapter 7
490(14)
Chapter 8
504(5)
Chapter 9
509(9)
Chapter 10
518(8)
References for figures 526(5)
Index 531

An electronic version of this book is available through VitalSource.

This book is viewable on PC, Mac, iPhone, iPad, iPod Touch, and most smartphones.

By purchasing, you will be able to view this book online, as well as download it, for the chosen number of days.

A downloadable version of this book is available through the eCampus Reader or compatible Adobe readers.

Applications are available on iOS, Android, PC, Mac, and Windows Mobile platforms.

Please view the compatibility matrix prior to purchase.